solution was injected on a Superdex

solution was injected on a Superdex™ 30 column (HiLoad™ Prep Grade, 26 x 600
mm). Elution with 0.15 M NH4HCO3 solution in flow rate of 2 mL/min, while monitoring at 184
nm, provided baseline separation between CB[7] (retention volume, Rv = 270~530 mL) and
iCB[7] (Rv = 660~890 mL). After evaluating the purity of selected fractions by 1H NMR spectra,
fractions were combined and lyophilized to obtain pure iCB[7] (69 mg).

結果 (中文) 1:

解决方案被注入 Superdex ™ 30 列 (抓取 ™ 预备级，26 x 600毫米).同时监测在 184 2 毫升/分钟，流量 0.15 M 以溶液洗脱nm，提供基线分离之间 CB [7] (保留体积，Rv = 270 ~ 530 毫升) 和iCB [7] (Rv = 660 ~ 890 毫升)。后 1 H 核磁共振谱，评估所选组分的纯度分数是结合并冻干以获得纯 iCB [7] (69 毫克)。

結果 (中文) 3:

溶液注入™Superdex 30柱（HiLoad™预备年级，26 x 600
毫米）。0.15米的NH4HCO3溶液在2毫升/分钟的流速洗脱，在184 nm
监测，提供CB [ 7 ]之间的基线分离（保留体积，RV = 270 ~ 530毫升）和
ICB [ 7 ]（RV = 660 ~ 890毫升）。通过核磁共振谱对所选组分的纯度进行评价组分结合，冻干得到纯ICB [ 7 ]（69毫克）。