X-ray diffractometer consists of three basic elements: X-ray tube, sample holder and the X-ray detector. By heating the filaments to produce electrons, and accelerating electrons by applying a voltage so that the target moves, and the electron striking the target material, thereby generating X-rays in the cathode ray tube. When the electrons have sufficient energy to inner-shell electron transfer target material, will have a characteristic X-ray spectroscopy. These spectra are composed of several components, the most common is the Kα and Kβ. Kα Kα1 and Kα2 in part by the composition. Kα1 slightly shorter wavelengths, intensity is twice the Kα2. Is characteristic of a particular wavelength of the target material. Need to be filtered or a crystal monochromator with foil to produce a desired monochromatic X-ray diffraction. Kα1 and Kα2 wavelengths close enough, it is possible to use a weighted average of both. Molybdenum is the most common single-crystal diffraction target material, MoKα radiation = 0.7107Å. These X-rays are collimated and directed to the sample. When the incident X-rays strike the sample geometry satisfy the Bragg equation, constructive interference occurs. Recording the detector and X-ray signal processing, and converts the signal to count rate, and outputs it to a printer or a computer monitor and other equipment. Synchrotron X-ray may also be used to generate the synchrotron beam emitted stronger.
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