The modified fly ash was studied in the treatment of lead containing wastewater,The fly ash were acid treatment;Alkali treatment; heat treatment;And the flux processing。The results show that high temperature treatment of modified fly ash removal effect than other modified equivalent。And the high temperature modified by orthogonal test experiment:Heat treatment temperature;The time of adsorption;The adsorption temperature;Wastewater PH;Upon adsorption temperature affect the lead containing wastewater by adsorption effect,To determine the optimal scheme for 900℃calcined,3G modified fly ash,Reaction of 40min,PH=7,The best effect at 25 ℃。