Smallest reaction to be attempted,

Smallest reaction to be attempted, especially by newbees, is 1oz of pfed! So that even taking into account sloppiness, lack of experience and losses along the way You should get some product!

Ratios of reagents are, 3:3:1 or 1:1:1/3 ie.E:I:RP aka, equal amounts of Iodine and pfed, and a third as much RP! Comprenda!

Ok first prepare yourself an icebath! Yes icecubes and water in a sink or bucket! Now, many will say you should add this first or that first! Well after much reading of different peoples methods, I say.... Chuck the whole shebang in together, while your flask is on ice, Lift and swirl ingredients together, while maintaing on ice! Put your condenser on top and start water running thru, from bottom to top! Now, the idea is to get the reaction going in the most controlled way possible. Now you want to let reagents react in the icebath, if at all, Then move vessel from icebath to room temp, If things look like they're going too fast, put back in ice bath, You want to keep the reaction going but only at a nice slow, controlled pace! This is also necessary to control vapour in the condenser! Thick and or dis-colored smoke is bad! and plumes of smoke will escape from condenser As things progress at a nice slow pace, as things slow too much you can start applying heat! So prepare an oilbath and bring to about 50c, now if there is no more action in your vessel You can move it to the oilbath, and same as before, when things slow down, Adjust heat up, to say 100c then 150c for one hour, to make sure reaction has completed The whole time you should be watching to keep a nice reflux going, and not too much vapour is escaping from condenser!

結果 (中文) 1:

最小的反应，特别是种的由 newbees，尝试是种的 1 盎司!所以，即使考虑到帐户草率、 缺乏经验和一路走来你应该得到一些产品的损失!比率的试剂是，3:3:1 或 1:1:1 / 3 即。E: 我: RP aka，等量的碘和种和第三个一样的 RP!Comprenda!好吧首先准备你自己的 icebath!是的 icecubes 和在一个水槽或水桶的水!现在，许多人会说你应该添加这一或那第一!好后不同民族方法多阅读，我说......把整个事情一起，而您的水壶是冰、 电梯和旋流成分在一起，同时在冰上的版权吧!把你的凝汽器放在上面，开始水中的跑步穿过，从底部到顶部!现在，这个想法是要在最可控的方式可能会反应。现在你想让试剂反应，在 icebath，如果在所有，然后将移动船只从 icebath 到室温，如果东西看起来像他们走得太快，放回冰浴，你想要维持反应的继续，但只在一个很好慢，控制步伐!这也是需要控制蒸汽在冷凝器中!厚和或解散彩色烟雾是坏的!和的浓烟将逃出冷凝器，随着事情的进展在好缓慢的步伐，因为事情慢太多你可以开始应用热!所以准备 oilbath，如果没有更多的行动带到 50 摄氏度，现在在你的船你可以将其移动到 oilbath，和相同当事情慢下来，调整加热，说一个小时，然后 150 c 100 c 之前，以确保反应已完成整个时间你应该看的节目以保持好回流并不太多的蒸气逃离凝汽器!