The LOD and LOQ for each phthalate was calculated at S/N value of 3 and 10. The LODs and the LOQs were 0.05 and 0.10 mg/kg for DAP, DIBP, DMP, DBP and DEHP, 0.10 and 0.25 mg/kg for DIDP and DINP, 0.02 and 0.05 mg/kg for the other 15 PAEs (Table 2). Moreover, these values are compatible with the expected values targeted in real samples.