The pattern of glycosyl linkages an

The pattern of glycosyl linkages and sequence of residues were determined by HMBC and ROESY (Fig. 4A). The 3-linkage was confirmed by the correlations from H-1 to C-3 in HMBC and the correlations from H-1 to H-3 in ROESY. Taking fraction II as an example, in its HMBC spectrum, a correlation from H-1 of residue B to C-3 of residue A’, H-1 of residue B to C-3 of residue A, a correlation from H-1 of residue C to C-3 of residue B, and a correlation from H-1 of residue D to C-3 of residue C were observed. In ROESY spectrum (Fig. 4A), a correlation from H-1 of residue B to H-3 of residue A0, H-1 of residue B to H-3 of residue A, a correlation from H-1 of residue C to H-3 of residue B, and a correlation from H-1 of residue

結果 (中文) 1:

糖基联系的模式和序列的残留量测定惠丰和 ROESY （图 4A）。3-连杆的牢固性由 C-3 在惠丰从 H 1 相关性和从 H 1 H-3 在 ROESY 中的相关性。以分数作为一个例子，在它的惠丰光谱相关性的残留 B 到 C-3 的滤渣 A H-1 二 '，H-1 H-1 的残留 D C-3 的残留物 C 观察从 B 到 C-3 滤渣 A、 H-1 的残留 B、 C 3 C 残留的相关性和相关残留。在 ROESY 谱 （图 4A），H-1 的残留 B H-3 的残留 A0，H-1 的残留 B H-3 滤渣 A、 H-1 H-3 的残留 B，C 残留量的相关性和 H-1 的残留物的相关性的相关性

結果 (中文) 3:

通过HMBC和ROESY测定糖基键序列的残基的模式（图4A）。这是fi3-linkage CON rmed从H-1的相关性，C-3 HMBC和相关H-1 H-3 ROESY。以组分II为例，在其HMBC谱，相关性H-1 B的渣渣的C-3，H-1 B C-3渣渣，相关的H-1残留C C-3残留B，和一个相关的H-1残留D C-3残留c的观察。在ROESY谱（图4a），相关的H-1残留B H-3残留A0，H-1 B H-3渣渣，相关从H-1残留C H-3残留B，和残留
h-1的相关性