To obtain nanocrystalline TiO2/ZnO,

To obtain nanocrystalline TiO2/ZnO, the following procedure was used. Liquid TiCl3 was dissolved in water in the desired concentration. Two milliliters of TiCl3 (20-30 wt % in HCl,
Aldrich Chemicals, U.S.A.) was added to an ice-cooled mixture consisting of 20 mL of deionized water (18 M¿ cm). The pH was adjusted to 3.0-3.5 using a 7% ammonium hydroxide solution with constant stirring. After stirring for 30 min, a homogeneous violet-black colored solution was obtained, which was stable for a period of several hours at room temperature.Clean indium tin oxide (ITO) substrates were floated on the surface of the dilute solution at room temperature (27 °C) to deposit a thin film. The solution became turbid after soaking for a period of about 15 min. After soaking for 6 h, the substrate was carefully rinsed with deionized water, ultrasonically cleaned with deionized water, and then dried under flowing argon gas.

結果 (中文) 1:

若要获得纳米 TiO2/ZnO，使用以下过程。液体 TiCl3 溶解在水中所需的浓度。两毫升的 TiCl3 （20-30 wt %的盐酸，奥尔德里奇化学品，美国）被添加到冰冷却混合物 20 毫升的去离子水 （18 M¿厘米）。Ph 值调整到 3.0-3.5 使用 7%氢氧化铵溶液不断搅拌。后搅拌 30min，均匀的紫黑色有色溶液制得，其中已经稳定了几个小时在室温。稀溶液在室温 (27 ° C)，沉积薄膜表面上漂浮了清洁铟氧化铟锡 (ITO) 衬底。溶液浸泡一段约 15 分钟后变得混浊。后浸泡 6 小时，承印物是仔细去离子水漂洗、 用去离子水、 超声清洗，然后晾干下流动氩气。

結果 (中文) 3:

获得纳米二氧化钛/氧化锌，以下程序使用。液以溶解在水中，在所需的浓度。两毫升三氯化钛（20-30 %盐酸，奥德里奇化工、美国）被添加到一个冰冷却由去离子水20毫升混合（18米¿厘米）。pH值调整到3.0-3.5用7%氢氧化铵溶液不断搅拌。搅拌30分钟后，得到均匀的紫黑色的解决方案，这一段在室温下几个小时是稳定的。干净的铟锡氧化物（ITO）衬底上的浮在表面的稀溶液在室温（27°C）沉积薄膜。浸泡时间约15分钟。浸泡6 h后溶液变浑浊，基板被小心地用去离子水漂洗，超声波去离子水清洗，然后晾干在流动的氩气。